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Amines and Aniline pH of aqueous ammonia, cyclohexylamine, and aniline, iodination of aniline, oxidation of aniline with benzoyl peroxide, the nitrous acid test, diazo coupling, reaction of luminol and light sticks are demonstrated.
Amines / Ammonium Compounds
Combustion Reactions Combustion reactions of methane, hydrogen, hexane, and natural gas in chlorine are demonstrated.
Reactions
Organic Compounds An assortment of organic compounds are ignited under various conditions.
A Pollutant Transformation Laboratory Exercise for Environmental Chemistry: The Reduction of Nitrobenzenes by Anaerobic Solutions of Humic AcidFrank M. Dunnivant and Mark-Cody Reynolds Presents a laboratory for advanced undergraduate- or graduate-level environmental chemistry in which students study the reduction of substituted nitrobenzenes by natural organic matter under anaerobic conditions. The exercise involves solution preparation, pH and EH buffers, organic reaction mechanisms, reaction kinetics, and instrumental analysis. Dunnivant, Frank M.; Reynolds, Mark-Cody. J. Chem. Educ.2007, 84, 315.
Instrumental Methods |
pH |
Solutions / Solvents |
Mechanisms of Reactions |
Kinetics |
Oxidation / Reduction
Diels–Alder Synthesis of endo-cis-N-Phenylbicyclo[2.2.2]oct-5-en-2,3-dicarboximideMarsha R. Baar and Kristin Wustholz endo-cis-N-Phenylbicyclo[2.2.2]oct-5-en-2,3-dicarboximide was synthesized by a DielsAlder cycloaddition of 1,3-cyclohexadiene and N-phenylmaleimide in ethyl acetate. 1,3-Cyclohexadiene and N-phenylmaleimide were selected to illustrate the Alder rule, which reflects a preference for endo products and to overcome the difficulties associated with the traditional combination of 1,3-cyclopentadiene and maleic anhydride. Baar, Marsha R.; Wustholz, Kristin. J. Chem. Educ.2005, 82, 1393.
Asymmetric Synthesis |
Microscale Lab |
Stereochemistry |
Addition Reactions |
Alkenes |
IR Spectroscopy |
NMR Spectroscopy
Microscale Synthesis of 1-Bromo-3-chloro-5-iodobenzene: An Improved Deamination of 4-Bromo-2-chloro-6-iodoanilineMichael W. Pelter, Libbie S.W. Pelter, Dusanka Colovic, and Regina Strug Overall, we find this procedure to be advantageous to the published methods owing to its requirement of less starting material, higher product yields, and a greatly simplified procedure. Pelter, Michael W.; Pelter, Libbie S.W.; Colovic, Dusanka; Strug, Regina. J. Chem. Educ.2004, 81, 111.
