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Using Ozone in Organic Chemistry Lab: The Ozonolysis of EugenolBruce M. Branan, Joshua T. Butcher, and Lawrence R. Olsen This organic laboratory involves the ozonolysis of eugenol (clove oil) followed by a reductive workup that generates an aldehyde easily identified by its NMR and IR spectra. Branan, Bruce M.; Butcher, Joshua T.; Olsen, Lawrence R. J. Chem. Educ.2007, 84, 1979.
Aldehydes / Ketones |
Gases |
IR Spectroscopy |
Laboratory Equipment / Apparatus |
Natural Products |
NMR Spectroscopy |
Synthesis |
Oxidation / Reduction
Probing the Rate-Determining Step of the Claisen–Schmidt Condensation by Competition ReactionsKendrew K. W. Mak, Wing-Fat Chan, Ka-Ying Lung, Wai-Yee Lam, Weng-Cheong Ng, and Siu-Fung Lee This article describes a physical organic experiment to identify the rate-determining step of the ClaisenSchmidt condensation of benzaldehyde and acetophenone by studying the linear free energy relationship. Mak, Kendrew K. W.; Chan, Wing-Fat; Lung, Ka-Ying; Lam, Wai-Yee; Ng, Weng-Cheong; Lee, Siu-Fung. J. Chem. Educ.2007, 84, 1819.
Aldehydes / Ketones |
Aromatic Compounds |
Gas Chromatography |
Kinetics |
Mechanisms of Reactions |
Synthesis
A Green Enantioselective Aldol Condensation for the Undergraduate Organic LaboratoryGeorge D. Bennett The proline-catalyzed aldol condensation between acetone and isobutyraldehyde proceeds in good yield and with high enantioselectivity at room temperature. This multi-week experiment also illustrates a number of principles and trade-offs of green chemistry. Bennett, George D. J. Chem. Educ.2006, 83, 1871.
