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A Solvent-Free Claisen Condensation Reaction for the Organic LaboratoryJohn J. Esteb and Matthew B. Stockton An experiment involving the Claisen condensation reaction for a first-year organic chemistry laboratory is presented. In this experiment, potassium tert-butoxide and ethyl phenylacetate are heated to 100 C for 30 minutes under solvent-free conditions to produce 2,4-diphenyl acetoacetate in 80% yield. Esteb, John J.; Stockton, Matthew B. J. Chem. Educ.2003, 80, 1446.
Synthesis |
Esters
Identification of an unknown ester: An analytical-organic experimentGrob, Robert L.; Husk, G. Ronald It is the student's challenge to hydrolyze an ester, separate and purify the resultant alcohol and acid, determine several physical and chemical characteristics, and arrive at a logical choice for its identity. Grob, Robert L.; Husk, G. Ronald J. Chem. Educ.1969, 46, 769.
Quantitative Analysis |
Esters |
Alcohols |
Carboxylic Acids
Recyclization apparatus for esterificationNaff, M. Benton; Naff, Anna S. Describes an apparatus and procedure involved in preparing and distilling n-butyl acetate. Naff, M. Benton; Naff, Anna S. J. Chem. Educ.1967, 44, 680.
Laboratory Equipment / Apparatus |
Esters
Other Resources: First 3 results
EstersEd Vitz, John W. Moore A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
Esters
Esters in FoodsRobert Hetue A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
Esters
Sodium Silicide Fueled BicyclesEd Vitz A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
