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Synthesis and Characterization of 9-Hydroxyphenalenone Using 2D NMR TechniquesBenjamin Caes and Dell Jensen Jr. The synthesis of 9-Hydroxyphenalenone produces a planar multicyclic beta-ketoenol, the tautomerization of which results in C2v symmetry on the NMR time scale, thus simplifying the spectra and providing a unique structure for teaching 2D NMR spectroscopy. Caes, Benjamin; Jensen, Dell, Jr. J. Chem. Educ.2008, 85, 413.
