12.1 Mass Spectrometry of Small Molecules: Magnetic-Sector Instruments
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Assessing Nitration Products of Benzene Derivatives Using TLC AnalysisRita K. Hessley Thin layer chromatography is applied to an earlier published, guided discovery experiment using GCMS analyses to identify isomers formed by the nitration of mono-substituted benzenes. Hessley, Rita K. J. Chem. Educ.2008, 85, 1623.
Thin Layer Chromatography |
Gas Chromatography |
Mass Spectrometry |
Aromatic Compounds
Identification of Secondary Metabolites in Citrus Fruit Using Gas Chromatography and Mass SpectroscopyJean-Michel Lavoie, Esteban Chornet, and André Pelletier Using a simple extraction and a gas chromatograph coupled with a mass spectrometer, this protocol allows students in analytical or organic chemistry to quantify and qualify monoterpenes from the peels of limes, grapefruits, and oranges. Lavoie, Jean-Michel; Chornet, Esteban; Pelletier, André. J. Chem. Educ.2008, 85, 1555.
Alkenes |
Food Science |
Gas Chromatography |
Mass Spectrometry |
Natural Products |
Plant Chemistry |
Qualitative Analysis |
Quantitative Analysis
The Iodochlorination of Styrene: An Experiment That Makes a DifferenceR. Gary Amiet and Sylvia Urban This purpose of this laboratory exercise is to determine the various substitution and elimination products generated in the iodochlorination of styrene and their relative proportions through the application of mechanistic principles and a basic knowledge of GCMS and NMR. Amiet, R. Gary; Urban, Sylvia. J. Chem. Educ.2008, 85, 962.
