11.10 Determining Crystal Structure by X-Ray Diffraction
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A-DNA and B-DNA: Comparing Their Historical X-ray Fiber Diffraction ImagesAmand A. Lucas This paper provides a comparative explanation of the structural content of the diffraction diagrams of A-DNA and B-DNA that facilitated the discovery of the double-helical structure of DNA by Watson and Crick in 1953. This analysis is supported a method that simulates both A-DNA and B-DNA X-ray images optically. Lucas, Amand A. J. Chem. Educ.2008, 85, 737.
Biophysical Chemistry |
Conformational Analysis |
Crystals / Crystallography |
X-ray Crystallography |
Nucleic Acids / DNA / RNA
Preparation and Characterization of Solid Co(II) Pyrimidinolates in a Multifaceted Undergraduate Laboratory ExperimentNorberto Masciocchi, Simona Galli, Angelo Sironi, Gabriella Dal Monte, Elisa Barea, Juan Manuel Salas, and Jorge A. R. Navarro Presents an integrated set of experiments involving the [Co(4-pyrimidinolate)2(H2O)n] species, including synthesis; analytical characterization by conventional titration and colorimetric methods; thermal, spectroscopic and structural characterization; and advanced analytical techniques (XRF, XRD). Masciocchi, Norberto; Galli, Simona; Sironi, Angelo; Dal Monte, Gabriella; Barea, Elisa; Salas, Juan Manuel; Navarro, Jorge A. R. J. Chem. Educ.2008, 85, 422.
