Instrumental Methods: Infrared Spectroscopy and Vibrations of Chemical Bonds
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Designing and Conducting a Purification Scheme as an Organic Chemistry Laboratory PracticalKate J. Graham, Brian J. Johnson, T. Nicholas Jones, Edward J. McIntee, and Chris P. Schaller Describes an open-ended laboratory practical that challenges students to evaluate when different purification techniques are appropriate. Graham, Kate J.; Johnson, Brian J.; Jones, T. Nicholas; McIntee, Edward J.; Schaller, Chris P. J. Chem. Educ.2008, 85, 1644.
IR Spectroscopy |
Microscale Lab |
Molecular Properties / Structure |
NMR Spectroscopy |
Physical Properties |
Separation Science
The Electrochemical Synthesis of Transition-Metal AcetylacetonatesS. R. Long, S. R. Browning, and J. J. Lagowski The electrochemical synthesis of transition-metal acetylacetonates can assist in the transformation of an entry-level laboratory course into a research-like environment where all members of a class are working on the same problem, but each student has a personal responsibility for the synthesis and characterization of a specific compound. Long, S. R.; Browning, S. R.; Lagowski, J. J. J. Chem. Educ.2008, 85, 1429.
The Spectra of Molecules: InfraredEd Vitz, John W. Moore A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
IR Spectroscopy
3D NormalModes Shockwave; A Web Application for Interactive Visualization and Three Dimensional PercNickolas D. Charistos, C. A. Tsipis, Michael P. Sigalas 3D Normal Modes is a Web application for interactive visualization and three-dimensional perception of the normal modes of molecular vibration, suitable for undergraduate students in chemistry. The application uses the Macromedia Shockwave plug-in and has been designed and developed especially for the Web. It has a simple graphical user interface and requires a download of only 120 KB, allowing it to be used even with low bandwidth Internet connections. Its performance is comparable to a desktop application.
IR Spectroscopy |
Raman Spectroscopy
The Effect of Anharmonicity on Diatomic Vibration; A Spreadsheet SimulationWilliam F. Coleman, Kieran F. Lim Instructors and students can use this spreadsheet to quickly and easily observe how the shape of a one-dimensional vibrational potential energy curve and its associated vibrational quantum energy levels depend on the anharmonicity. This illustrates the connection between the harmonic (approximation) and anharmonic descriptions of molecular vibrations.