17.3. What Are the Physical Properties of Aldehydes and Ketones?, 461
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Borohydride Reduction of EstroneAnimesh Aditya, David E. Nichols, and G. Marc Loudon This experiment presents a guided-inquiry approach to the demonstration of diastereoselectivity using chiral hindered ketones that undergo facile reduction with sodium borohydride. The resulting diastereomeric estradiols can be analyzed and differentiated by thin-layer chromatography and melting point. Aditya, Animesh; Nichols, David E.; Loudon, G. Marc. J. Chem. Educ.2008, 85, 1535.
Aldehydes / Ketones |
Diastereomers |
IR Spectroscopy |
Microscale Lab |
Stereochemistry |
Steroids |
Thin Layer Chromatography
Facing the Music: How Original Was Borodin's Chemistry?Michael D. Gordin A return to the original sources demonstrates that the evidence for Borodin's reputation as a great chemist, as opposed to a merely good one, is exaggerated. Gordin, Michael D. J. Chem. Educ.2006, 83, 561.
Aldehydes / Ketones |
Amines / Ammonium Compounds |
Enrichment / Review Materials |
Nonmajor Courses
Methyl Ethyl KetoneJay A. Young The hazards of methyl ethyl ketone are described. Young, Jay A. J. Chem. Educ.2004, 81, 630.
