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Phenols and Quinones Ferric chloride test for phenols, nitration of acetaminophen, extraction of dichloroindophenol, oxidation of phenols with sodium periodate, nucleophilic addition to quinones, "purple benzene", oxidation of 2,6-Dit-butlhydoquinone, decolorization of crystal violet, and chameleon emulsion are demonstrated.
A Bioanalytical Chemistry Experiment for Undergraduate Students: Biosensors Based on Metal NanoparticlesJohn Njagi, John Warner, and Silvana Andreescu Describes a laboratory experiment on the development of a biosensor in which students apply electrochemical methods to deposit gold nanoparticles onto electrode surfaces, immobilize an enzyme using glutaraldehyde chemistry, and perform quantitative analysis of phenol using a biosensor with amperometric detection. Njagi, John; Warner, John; Andreescu, Silvana. J. Chem. Educ.2007, 84, 1180.
Bioanalytical Chemistry |
Electrochemistry |
Enzymes |
Oxidation / Reduction |
Phenols
PhenolJay A. Young Safety precautions for handling phenol are discussed. Young, Jay A. J. Chem. Educ.2007, 84, 759.
Phenols |
Laboratory Management
The Base-Induced Reaction of Salicylaldehyde with 1-Bromobutane in Acetone: Two Related Examples of Chemical Problem SolvingHolly D. Bendorf and Chriss E. McDonald Each student performs his or her own experimental work, running one of the two reactions, and acquiring the proton and carbon NMR, IR, and mass spectra. The students work in groups to propose structures for the products and mechanisms for their formation. The students are also asked to address why the reactions take different courses. Bendorf, Holly D.; McDonald, Chriss E. J. Chem. Educ.2003, 80, 1185.
