12.4. What Are the Physical Properties of Alkenes and Alkynes?, 361
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Reactions: Acetylene Preparation of acetylene and the reaction of chlorine with acetylene are demonstrated. An antique carbide lamp is also demonstrated.
Identification of Secondary Metabolites in Citrus Fruit Using Gas Chromatography and Mass SpectroscopyJean-Michel Lavoie, Esteban Chornet, and André Pelletier Using a simple extraction and a gas chromatograph coupled with a mass spectrometer, this protocol allows students in analytical or organic chemistry to quantify and qualify monoterpenes from the peels of limes, grapefruits, and oranges. Lavoie, Jean-Michel; Chornet, Esteban; Pelletier, André. J. Chem. Educ.2008, 85, 1555.
Alkenes |
Food Science |
Gas Chromatography |
Mass Spectrometry |
Natural Products |
Plant Chemistry |
Qualitative Analysis |
Quantitative Analysis
Diels–Alder Synthesis of endo-cis-N-Phenylbicyclo[2.2.2]oct-5-en-2,3-dicarboximideMarsha R. Baar and Kristin Wustholz endo-cis-N-Phenylbicyclo[2.2.2]oct-5-en-2,3-dicarboximide was synthesized by a DielsAlder cycloaddition of 1,3-cyclohexadiene and N-phenylmaleimide in ethyl acetate. 1,3-Cyclohexadiene and N-phenylmaleimide were selected to illustrate the Alder rule, which reflects a preference for endo products and to overcome the difficulties associated with the traditional combination of 1,3-cyclopentadiene and maleic anhydride. Baar, Marsha R.; Wustholz, Kristin. J. Chem. Educ.2005, 82, 1393.
Asymmetric Synthesis |
Microscale Lab |
Stereochemistry |
Addition Reactions |
Alkenes |
IR Spectroscopy |
NMR Spectroscopy
Fractional Distillation and GC Analysis of Hydrocarbon MixturesCraig J. Donahue Separating and identifying the components of a three-hydrocarbon mixture through fractional distillation and gas chromatography. Donahue, Craig J. J. Chem. Educ.2002, 79, 721.
