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Diastereoselectivity in the Reduction of α-Hydroxyketones. An Experiment for the Chemistry Major Organic LaboratoryDavid B. Ball Describes a research type, inquiry-based project where students synthesize racemic ahydroxyketones using umpolung, a polarity-reversal approach; investigate chelating versus non-chelating reducing agents; and determine the diastereoselectivity of these reducing processes by NMR spectroscopy. Ball, David B. J. Chem. Educ.2006, 83, 101.
Addition Reactions |
Aldehydes / Ketones |
Chirality / Optical Activity |
Chromatography |
Conferences |
Constitutional Isomers |
Enantiomers |
NMR Spectroscopy |
Stereochemistry |
Synthesis |
Conformational Analysis
Benzoin Condensation: Monitoring a Chemical Reaction by High-Pressure Liquid ChromatographyApurba Bhattacharya, Vikram C. Purohit, and Nicholas R. Beller High-pressure liquid chromatography was successfully introduced in the undergraduate advanced organic chemistry laboratory to reinvestigate the cyanide-catalyzed condensation of benzaldehyde to benzoin. Bhattacharya, Apurba; Purohit, Vikram C.; Beller, Nicholas R. J. Chem. Educ.2004, 81, 1020.
