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For the textbook, chapter, and section you specified we found
7 Videos
27 Journal Articles
2 Other Resources
Videos: First 3 results
Recrystallization procedures using a single solvent and using two solvents are demonstrated.
Laboratory Equipment / Apparatus |
Separation Science
Separating and Purifying  
Laboratory processes frequently used to separate mixtures or purify substances including centrifuging, chromatography, distillation, extraction, filtration, and recrystallization are demonstrated.
Laboratory Equipment / Apparatus |
Separation Science
Centrifuging a Sample  John W. Moore, Jerrold J. Jacobsen, Lois M. Browne, John F. Zimmerman
The demonstration on this page shows a technique that should not be used by undergraduate chemistry laboratory. This video shows what happens to sample in a centrifuge while the centrifuge is on, and the result of stopping the centrifuge improperly. A narrative is included in this video: The centrifuging process allows the solvent to completely settle out. The jarring caused by hand braking destroys the distinct separation between supernatant and solid.
Separation Science |
Laboratory Equipment / Apparatus
View all 7 results
Journal Articles: First 3 results.
Designing and Conducting a Purification Scheme as an Organic Chemistry Laboratory Practical  Kate J. Graham, Brian J. Johnson, T. Nicholas Jones, Edward J. McIntee, and Chris P. Schaller
Describes an open-ended laboratory practical that challenges students to evaluate when different purification techniques are appropriate.
Graham, Kate J.; Johnson, Brian J.; Jones, T. Nicholas; McIntee, Edward J.; Schaller, Chris P. J. Chem. Educ. 2008, 85, 1644.
IR Spectroscopy |
Microscale Lab |
Molecular Properties / Structure |
NMR Spectroscopy |
Physical Properties |
Separation Science
The Resolution of Ibuprofen, 2-(4′-Isobutylphenyl)propionic Acid  James V. McCullagh
In this experiment the over-the-counter pain reliever ibuprofen is resolved using (S)-(-)-a-phenethylamine as the resolving agent. This procedure has several key advantages over previous resolution experiments.
McCullagh, James V. J. Chem. Educ. 2008, 85, 941.
Chirality / Optical Activity |
Drugs / Pharmaceuticals |
Enantiomers |
Quantitative Analysis |
Separation Science
Using a Simulated Industrial Setting for the Development of an Improved Solvent System for the Recrystallization of Benzoic Acid: A Student-Centered Project  Timothy R. Hightower and Jay D. Heeren
Presents a peer-led, problem-solving organic laboratory exercise that provide students with an opportunity to produce a more efficient recrystallization solvent in an industrial environment.
Hightower, Timothy R.; Heeren, Jay D. J. Chem. Educ. 2006, 83, 1663.
Carboxylic Acids |
Industrial Chemistry |
Separation Science |
Solutions / Solvents
View all 27 articles
Other Resources: 2 results
The Separation of Mixtures  Ed Vitz, John W. Moore
A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
Separation Science
Distillation  Ed Vitz, John W. Moore
A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
Physical Properties |
Separation Science