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Diastereoselectivity in the Reduction of α-Hydroxyketones. An Experiment for the Chemistry Major Organic LaboratoryDavid B. Ball Describes a research type, inquiry-based project where students synthesize racemic ahydroxyketones using umpolung, a polarity-reversal approach; investigate chelating versus non-chelating reducing agents; and determine the diastereoselectivity of these reducing processes by NMR spectroscopy. Ball, David B. J. Chem. Educ.2006, 83, 101.
Addition Reactions |
Aldehydes / Ketones |
Chirality / Optical Activity |
Chromatography |
Conferences |
Constitutional Isomers |
Enantiomers |
NMR Spectroscopy |
Stereochemistry |
Synthesis |
Conformational Analysis
A source of isomer-drawing assignmentsKjonaas, Richard A. A comprehensive source from which instructors can choose a wide variety of good isomer drawing examples to use as homework assignments and exam questions. Kjonaas, Richard A. J. Chem. Educ.1992, 69, 452.
Stereochemistry |
Alcohols |
Alkanes / Cycloalkanes |
Alkenes |
Aldehydes / Ketones |
Ethers |
Esters |
Alkynes
Selective oxidation in the presence of a heterocycleBowles, K. Dean; Quincy, David A.; McKenna, John I.; Natale, N. R. The process of weighing the advantages and disadvantages of various oxidation methods are presented in this paper. Bowles, K. Dean; Quincy, David A.; McKenna, John I.; Natale, N. R. J. Chem. Educ.1986, 63, 358.
