14.4. Mass Spectrometry in the Organic Synthesis Laboratory and Other Applications
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Synthesis of DiapocyninMina S. Dasari, Kristy M. Richards, Mikaela L. Alt, Clark F. P. Crawford, Amanda Schleiden, Jai Ingram, Abdel Aziz Amadou Hamidou, Angela Williams, Patricia A. Chernovitz, Rensheng Luo, Grace Y. Sun, Ron Luchtefeld, and Robert E. Smith Diapocynin is synthesized by the oxidative coupling of apocynin and analyzed by FTIR, 1H NMR, and negative ion atmospheric pressure chemical ionization LCMS. Dasari, Mina S.; Richards, Kristy M.; Alt, Mikaela L.; Crawford, Clark F. P.; Schleiden, Amanda; Ingram, Jai; Hamidou, Abdel Aziz Amadou; Williams, Angela; Chernovitz, Patricia A.; Luo, Rensheng; Sun, Grace Y.; Luchtefeld, Ron; Smith, Robert E. J. Chem. Educ.2008, 85, 411.
Drugs / Pharmaceuticals |
HPLC |
Mass Spectrometry |
Phenols |
Synthesis
Microwave-Assisted Organic Synthesis in the Organic Teaching Lab: A Simple, Greener Wittig ReactionEric Martin and Cynthia Kellen-Yuen A microwave-assisted Wittig reaction has been developed for the organic teaching laboratory. Utilizing this technique, a variety of styrene derivatives have been synthesized from aromatic aldehydes in good yields. The mixture of cis and trans alkenes produced also provides instructors with opportunities to emphasize the spectroscopic analysis of product mixtures. Martin, Eric; Kellen-Yuen, Cynthia. J. Chem. Educ.2007, 84, 2004.
