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NMR Determination of Internal Rotation Rates and Rotational Energy Barriers: A Physical Chemistry Lab ProjectKevin F. Morris and Luther E. Erickson This experiment will expose students to a variety of NMR techniques, such as saturation transfer, inversion-recovery, and line shape analysis. It will also demonstrate that NMR is an extremely useful tool to chemists, with very relevant applications in physical chemistry. Morris, Kevin F.; Erickson, Luther E. J. Chem. Educ.1996, 73, 471.
NMR Spectroscopy |
Instrumental Methods |
Chemometrics
Using Fourier Transforms to Understand Spectral Line ShapesGrunwald, Ernest; Herzog, Jonathan; Steel, Colin Using a computerized Fast Fourier Transforms (FFT) algorithm to analyze the rates of physical and chemical processes through dynamic spectroscopy. Grunwald, Ernest; Herzog, Jonathan; Steel, Colin J. Chem. Educ.1995, 72, 210.
Mechanisms That Interchange Axial and Equatorial Atoms in Fluxional ProcessesMarion E. Cass, Henry S. Rzepa, King Kuok Hii The Berry pseudorotation is a classical mechanism for interchanging axial and equatorial ligands in molecules with trigonal bipyramidal geometry. Teaching this mechanism presents particular pedagogic problems due to both its dynamic and three dimensional character. The approach taken here illustrates these processes using interactive animations embedded in a Web page and overcomes many limitations of a printed page.
