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Phenols and Quinones Ferric chloride test for phenols, nitration of acetaminophen, extraction of dichloroindophenol, oxidation of phenols with sodium periodate, nucleophilic addition to quinones, "purple benzene", oxidation of 2,6-Dit-butlhydoquinone, decolorization of crystal violet, and chameleon emulsion are demonstrated.
"Greening Up" the Suzuki ReactionEvangelos Aktoudianakis, Elton Chan, Amanda R. Edward, Isabel Jarosz, Vicki Lee, Leo Mui, Sonya S. Thatipamala, and Andrew P. Dicks This article describes the green synthesis of a biaryl compound via a Pd(0)-catalyzed Suzuki cross-coupling reaction in water. The methodology exposes students to purely aqueous microscale organic reactivity and showcases topical research regarding an industrial process. Aktoudianakis, Evangelos; Chan, Elton; Edward, Amanda R.; Jarosz, Isabel; Lee, Vicki; Mui, Leo; Thatipamala, Sonya S.; Dicks, Andrew P. J. Chem. Educ.2008, 85, 555.
Aromatic Compounds |
Catalysis |
Green Chemistry |
Microscale Lab |
Phenols |
Water / Water Chemistry
Synthesis of DiapocyninMina S. Dasari, Kristy M. Richards, Mikaela L. Alt, Clark F. P. Crawford, Amanda Schleiden, Jai Ingram, Abdel Aziz Amadou Hamidou, Angela Williams, Patricia A. Chernovitz, Rensheng Luo, Grace Y. Sun, Ron Luchtefeld, and Robert E. Smith Diapocynin is synthesized by the oxidative coupling of apocynin and analyzed by FTIR, 1H NMR, and negative ion atmospheric pressure chemical ionization LCMS. Dasari, Mina S.; Richards, Kristy M.; Alt, Mikaela L.; Crawford, Clark F. P.; Schleiden, Amanda; Ingram, Jai; Hamidou, Abdel Aziz Amadou; Williams, Angela; Chernovitz, Patricia A.; Luo, Rensheng; Sun, Grace Y.; Luchtefeld, Ron; Smith, Robert E. J. Chem. Educ.2008, 85, 411.
Drugs / Pharmaceuticals |
HPLC |
Mass Spectrometry |
Phenols |
Synthesis
A Bioanalytical Chemistry Experiment for Undergraduate Students: Biosensors Based on Metal NanoparticlesJohn Njagi, John Warner, and Silvana Andreescu Describes a laboratory experiment on the development of a biosensor in which students apply electrochemical methods to deposit gold nanoparticles onto electrode surfaces, immobilize an enzyme using glutaraldehyde chemistry, and perform quantitative analysis of phenol using a biosensor with amperometric detection. Njagi, John; Warner, John; Andreescu, Silvana. J. Chem. Educ.2007, 84, 1180.
