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Phenols and Quinones Ferric chloride test for phenols, nitration of acetaminophen, extraction of dichloroindophenol, oxidation of phenols with sodium periodate, nucleophilic addition to quinones, "purple benzene", oxidation of 2,6-Dit-butlhydoquinone, decolorization of crystal violet, and chameleon emulsion are demonstrated.
"Greening Up" the Suzuki ReactionEvangelos Aktoudianakis, Elton Chan, Amanda R. Edward, Isabel Jarosz, Vicki Lee, Leo Mui, Sonya S. Thatipamala, and Andrew P. Dicks This article describes the green synthesis of a biaryl compound via a Pd(0)-catalyzed Suzuki cross-coupling reaction in water. The methodology exposes students to purely aqueous microscale organic reactivity and showcases topical research regarding an industrial process. Aktoudianakis, Evangelos; Chan, Elton; Edward, Amanda R.; Jarosz, Isabel; Lee, Vicki; Mui, Leo; Thatipamala, Sonya S.; Dicks, Andrew P. J. Chem. Educ.2008, 85, 555.
Aromatic Compounds |
Catalysis |
Green Chemistry |
Microscale Lab |
Phenols |
Water / Water Chemistry
A Bioanalytical Chemistry Experiment for Undergraduate Students: Biosensors Based on Metal NanoparticlesJohn Njagi, John Warner, and Silvana Andreescu Describes a laboratory experiment on the development of a biosensor in which students apply electrochemical methods to deposit gold nanoparticles onto electrode surfaces, immobilize an enzyme using glutaraldehyde chemistry, and perform quantitative analysis of phenol using a biosensor with amperometric detection. Njagi, John; Warner, John; Andreescu, Silvana. J. Chem. Educ.2007, 84, 1180.
Bioanalytical Chemistry |
Electrochemistry |
Enzymes |
Oxidation / Reduction |
Phenols
Enthalpy of Vaporization and Vapor Pressures: An Inexpensive ApparatusRubin Battino, David A. Dolson, Michael R. Hall, and Trevor M. Letcher Describes an inexpensive apparatus for the determination of the vapor pressure of a liquid as a function of temperature for the purpose of calculating enthalpy changes of vaporization. Also described are a simple air thermostat and an inexpensive temperature controller based on an integrated temperature sensor. Battino, Rubin; Dolson, David A.; Hall, Michael R.; Letcher, Trevor M. J. Chem. Educ.2007, 84, 822.
