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Phenols and Quinones Ferric chloride test for phenols, nitration of acetaminophen, extraction of dichloroindophenol, oxidation of phenols with sodium periodate, nucleophilic addition to quinones, "purple benzene", oxidation of 2,6-Dit-butlhydoquinone, decolorization of crystal violet, and chameleon emulsion are demonstrated.
Synthesis of DiapocyninMina S. Dasari, Kristy M. Richards, Mikaela L. Alt, Clark F. P. Crawford, Amanda Schleiden, Jai Ingram, Abdel Aziz Amadou Hamidou, Angela Williams, Patricia A. Chernovitz, Rensheng Luo, Grace Y. Sun, Ron Luchtefeld, and Robert E. Smith Diapocynin is synthesized by the oxidative coupling of apocynin and analyzed by FTIR, 1H NMR, and negative ion atmospheric pressure chemical ionization LCMS. Dasari, Mina S.; Richards, Kristy M.; Alt, Mikaela L.; Crawford, Clark F. P.; Schleiden, Amanda; Ingram, Jai; Hamidou, Abdel Aziz Amadou; Williams, Angela; Chernovitz, Patricia A.; Luo, Rensheng; Sun, Grace Y.; Luchtefeld, Ron; Smith, Robert E. J. Chem. Educ.2008, 85, 411.
Drugs / Pharmaceuticals |
HPLC |
Mass Spectrometry |
Phenols |
Synthesis
A Bioanalytical Chemistry Experiment for Undergraduate Students: Biosensors Based on Metal NanoparticlesJohn Njagi, John Warner, and Silvana Andreescu Describes a laboratory experiment on the development of a biosensor in which students apply electrochemical methods to deposit gold nanoparticles onto electrode surfaces, immobilize an enzyme using glutaraldehyde chemistry, and perform quantitative analysis of phenol using a biosensor with amperometric detection. Njagi, John; Warner, John; Andreescu, Silvana. J. Chem. Educ.2007, 84, 1180.
Bioanalytical Chemistry |
Electrochemistry |
Enzymes |
Oxidation / Reduction |
Phenols
PhenolJay A. Young Safety precautions for handling phenol are discussed. Young, Jay A. J. Chem. Educ.2007, 84, 759.
