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Cocrystal Controlled Solid-State SynthesisMiranda L. Cheney, Michael J. Zaworotko, Steve Beaton, and Robert D. Singer Describes experiments that can easily be adapted to a typical undergraduate organic chemistry course and are inexpensive, relatively safe, require little or no solvent, have high atom economy, make use of non-toxic or low toxicity compounds, and generate negligible quantities of waste. Cheney, Miranda L.; Zaworotko, Michael J.; Beaton, Steve; Singer, Robert D. J. Chem. Educ.2008, 85, 1649.
Amines / Ammonium Compounds |
Calorimetry / Thermochemistry |
Green Chemistry |
IR Spectroscopy |
Microscale Lab |
Solid State Chemistry |
Synthesis
Preparation of a N-Heterocyclic Carbene Nickel(II) ComplexVincent Ritleng, Eric Brenner, and Michael J. Chetcuti Describes a four-part experiment that provides an excellent example of N-heterocyclic carbeneligand preparation and its subsequent complexation to a transition metal, as well as opportunities for students to learn standard Schlenk techniques and characterize products through 1H NMR spectroscopy. Ritleng, Vincent; Brenner, Eric; Chetcuti, Michael J. J. Chem. Educ.2008, 85, 1646.
The Spectra of Molecules: InfraredEd Vitz, John W. Moore A section of ChemPrime, the Chemical Educations Digital Library's free General Chemistry textbook.
IR Spectroscopy
3D NormalModes Shockwave; A Web Application for Interactive Visualization and Three Dimensional PercNickolas D. Charistos, C. A. Tsipis, Michael P. Sigalas 3D Normal Modes is a Web application for interactive visualization and three-dimensional perception of the normal modes of molecular vibration, suitable for undergraduate students in chemistry. The application uses the Macromedia Shockwave plug-in and has been designed and developed especially for the Web. It has a simple graphical user interface and requires a download of only 120 KB, allowing it to be used even with low bandwidth Internet connections. Its performance is comparable to a desktop application.
IR Spectroscopy |
Raman Spectroscopy
The Effect of Anharmonicity on Diatomic Vibration; A Spreadsheet SimulationWilliam F. Coleman, Kieran F. Lim Instructors and students can use this spreadsheet to quickly and easily observe how the shape of a one-dimensional vibrational potential energy curve and its associated vibrational quantum energy levels depend on the anharmonicity. This illustrates the connection between the harmonic (approximation) and anharmonic descriptions of molecular vibrations.
