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Identification of Secondary Metabolites in Citrus Fruit Using Gas Chromatography and Mass SpectroscopyJean-Michel Lavoie, Esteban Chornet, and André Pelletier Using a simple extraction and a gas chromatograph coupled with a mass spectrometer, this protocol allows students in analytical or organic chemistry to quantify and qualify monoterpenes from the peels of limes, grapefruits, and oranges. Lavoie, Jean-Michel; Chornet, Esteban; Pelletier, André. J. Chem. Educ.2008, 85, 1555.
Alkenes |
Food Science |
Gas Chromatography |
Mass Spectrometry |
Natural Products |
Plant Chemistry |
Qualitative Analysis |
Quantitative Analysis
NMR and IR Spectroscopy for the Structural Characterization of Edible Fats and OilsMolly W. Crowther This article describes an upper-level instrumental laboratory for undergraduates that explores the complementary nature of IR and NMR spectroscopy in the analysis of five edible and structurally similar fats and oils for average chain length, degree of unsaturation, and trans fat content. Crowther, Molly W. J. Chem. Educ.2008, 85, 1550.
Consumer Chemistry |
Food Science |
IR Spectroscopy |
NMR Spectroscopy |
Qualitative Analysis |
Spectroscopy |
Fatty Acids
The Synthesis of a Cockroach PheromonePatty L. Feist This paper describes the synthesis of gentisyl quinone isovalerate or blattellaquinone, a sex pheromone of the German cockroach and a compound with real-world applications. The experiment also affords students practice in extraction as well as IR and NMR spectroscopy. Feist, Patty L. J. Chem. Educ.2008, 85, 1548.
